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21. Structure of polypyrrole.

This synthetic method [451-461] regiospecifically generates 2-bromo-5-(bromomagnesio)-3-alkylseries of other metal-catalyzed couplings have been explored. thiophene, which is subsequently polymerized with catalytic amounts of Ni(dppp)Cl2 on the basis of the method reported Ni-Catalyzed Coupling Reactions Yamamoto Method. Yamamoto et al. [423] prepared polythio- by Tamao et al. [263] (Fig. 16). The method reported by Tamao phene by treating 2,5-dibromothiophene with Mg and catalyz- et al. [263] is also the basis for the Yamamoto procedure [258] ing the polymerization by Ni(bipyridine)2Cl2 (Fig.

16. McCullough method for regiospecific synthesis of poly(3alkylthiophene)s with 100% head-to-tail couplings. metal-catalyzed polycondensation reaction was reported by Lin and Dudek [424]. These methods are based on the coupling of Cu / PdClg Grignard reagents with aryl haUdes reported by Tamao et al. [263]. d) CIHg—^ >-HgCI Systematic studies of the polymerization of 2,5-dihalothiophene pyridine were performed by the group of Yamamoto, as well as by many other groups [259-263]. Varying the amounts of Mg, solvent, type of metal, monomer concentration, type of halogen on the thiophene, temperature, reaction time, and type of catalyst led to some Electrochem.

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