By J. Lawrynowicz, J. Lodz
Textual content: English, French
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Extra info for Analytic Functions, Blazejewko 1982
This procedure is not only very time consuming, but the more troublesome eﬀect is that the system cannot be used for analysis while the ﬂuid is being changed. Unfortunately, a leakage cannot always be avoided, especially if a new column is installed and the ﬁttings are not properly connected. 2. To conclude this section both from a practical perspective as well as from a technical standpoint, a device which is based on contact heating seems to be the best option in order to allow for a rapid and precise preheating of the eluent.
A reasonable explanation can be given when the systems which were used in these studies are compared. While Fields used a Gilson 831 column oven based on forced-air convection, we used a block-heating oven with the preheating capillary tightly clamped between two aluminium blocks. In addition, our View Article Online 28 Chapter 3 experimental results are in good agreement with the mathematical treatment of Abbott and co-workers. 5 cm long tubing. It can be summarized that heat transfer is most eﬀective if contact heating is used.
I have to stress that up until now no ‘‘intelligent’’ heating device exists which takes all variables into account and adjusts the eluent temperature accordingly. At this point more eﬀort has to be devoted to put such a system into practice. However, with some of the most advanced heating systems currently on the market, this aim could be achieved in the near future. 3 Technical Implementation of Eluent Preheating There are many ways to carry out eluent preheating and I would like to stress that it is not possible to consider all technical solutions.
Analytic Functions, Blazejewko 1982 by J. Lawrynowicz, J. Lodz